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Article Navigation >  PETROLEUM GEOLOGY & EXPERIMENT  > 2015  >  37(4): 525-529
Wang Liang, Zhang Xiongdong, Cao Haihong. Shale preparation using Ar-ion milling[J]. PETROLEUM GEOLOGY & EXPERIMENT, 2015, 37(4): 525-529. doi: 10.11781/sysydz201504525
Citation: Wang Liang, Zhang Xiongdong, Cao Haihong. Shale preparation using Ar-ion milling[J]. PETROLEUM GEOLOGY & EXPERIMENT, 2015, 37(4): 525-529. doi: 10.11781/sysydz201504525
shu

Shale preparation using Ar-ion milling

doi: 10.11781/sysydz201504525

  • Research Institute of Petroleum Exploration and Development, SINOPEC East China Company, Yangzhou, Jiangsu 225007, China

  • Received Date: 2014-07-11
  • Rev Recd Date: 2015-06-06
  • Publish Date: 2015-07-28
    Abstract
  • There are many micropores in shale, and the micropore structures can be exposed by Ar-ion milling technology. An Ar-ion beam was applied to treat a cross-section of shale with variable acceleration voltage, milling time, incidence angle and rotation speed of the sample holder. The milling effects were observed with a scanning electron microscope (SEM). The results show that appropriately lower voltage makes a smoother milling surface, and there is an optimal milling time. Meanwhile, a higher incidence angle and lower rotation speed of the holder can improve the milling effects.

     

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