Field testing technology for shale gas content
-
摘要: 对自行研发的智能化页岩气现场解吸系统进行改进,在解吸罐的内部加装温度传感器,监测罐内空间的温度,消除温度变化引起的气体体积膨胀对实验结果的影响。利用改进后的仪器对常规解吸方法进行了优化,提出以90℃或者110℃作为二阶解吸温度的高温解吸方法,可将测试时间从40 h缩短至12~25 h,在保证了测试结果可靠性的同时,具备实用性和安全性的优点。由于人工操作的影响,初期的解吸速率总会出现异常高点,针对这种情况,提出将岩心封罐之后的5 min解吸数据点作为损失气拟合时的初始点。Abstract: The in-house developed intelligent shale gas desorption system was improved. A temperature sensor was installed inside the desorption canister to monitor the interior temperature and eliminate the influence of gas volume expansion caused by temperature change on experimental results. The conventional desorption method was optimized by using the improved instrument. The high temperature desorption method at 90℃ or 110℃ as the second-order desorption temperature was proposed to shorten test time from 40 h to 12-25 h, which ensured the reliability of test results with the advantages of practicality and safety. Due to the influence of manual operation, the initial desorption rate would always be abnormally high. In this case, we advised the use of the desorption data 5 min after core sealing as the initial point when fitting gas loss curves.
-
Key words:
- temperature /
- desorption at high temperature /
- loss of gas /
- shale gas
-
[1] BOWKER K A.Barnett shale gas production,Fort Worth Basin:Issues and discussion[J].APPG Bulletin,2007,91(4):523-533. [2] ROSS D J K,BUSTIN R M.Characterizing the shale gas resource potential of Devonian-Mississippian strata in the western Canada sedimentary basin:Application of an integrated formation evaluation[J].APPG Bulletin,2008,92(1):87-125. [3] 李艳丽.页岩气储量计算方法探讨[J].天然气地球科学,2009,20(3):466-470. LI Yanli.Calculation methods of shale gas reserves[J].Natural Gas Geoscience,2009,20(3):466-470. [4] 王飞宇,贺志勇,孟晓辉,等.页岩气赋存形式和初始原地气量(OGIP)预测技术[J].天然气地球科学,2011,22(3):501-510. WANG Feiyu,HE Zhiyong,MENG Xiaohui,et al.Occurrence of shale gas and prediction of original gas in-place (OGIP)[J].Natural Gas Geoscience,2011,22(3):501-510. [5] 陈康,张金川,唐玄.湘鄂西下志留统龙马溪组页岩含气性测井评价[J].特种油气藏,2016,23(1):16-20. CHEN Kang,ZHANG Jinchuan,TANG Xuan.Gas content logging evaluation of Lower Silurian Longmaxi shale in western Hunan-Hubei[J].Special OiL & Gas Reservoirs,2016,23(1):16-20. [6] 张茂林,袁恩,梅海燕,等.新型页岩气藏物质平衡方程[J].断块油气田,2017,24(3):396-400. ZHANG Maolin,YUAN En,MEI Haiyan,et al.New material balance equation for shale gas reservoir[J].Fault-Block Oil and Gas Field,2017,24(3):396-400. [7] 陈元千,周翠.中国《页岩气资源/储量计算与评价技术规范》计算方法存在的问题与建议[J].油气地质与采收率,2015,22(1):1-4. CHEN Yuanqian,ZHOU Cui.Problems and recommendations for the Regulation of shale gas resources/reserves estimation in China[J].Petroleum Geology and Recovery Efficiency,2015,22(1):1-4. [8] 邢雅文,张金川,冯赫青,等.页岩含气量测试方法改进效果分析[J].断块油气田,2015,22(5):579-583. XING Yawen,ZHANG Jinchuan,FENG Heqing,et al.Effectiveness analysis of determination method for shale gas content[J].Fault-Block Oil and Gas Field,2015,22(5):579-583. [9] 包兴,李少华,张程,等.基于试验设计的概率体积法在页岩气储量计算中的应用[J].断块油气田,2017,24(5):678-681. BAO Xing,LI Shaohua,ZHANG Cheng,et al.Application of probability volume method based on experimental design to calculation of shale gas reserves[J].Fault-Block Oil and Gas Field,2017,24(5):678-681. [10] 国家能源局.SY/T 6940-2013,页岩含气量测定方法[S].北京:石油工业出版社,2014. National Energy Administration.SY/T 6940-2013,Measurement method of shale gas content[S].Beijing:Petroleum Industry Press,2014. [11] 刘洪林,邓泽,刘德勋,等.页岩含气量测试中有关损失气量估算方法[J].石油钻采工艺,2010,32(S1):156-158. LIU Honglin,DENG Ze,LIU Dexun,et al.Discussion on lost gas calculating methods in shale gas content testing[J].Oil Drilling & Production Technology,2010,32(S1):156-158. [12] 游声刚,郭茜,耿小烬,等.页岩含气量的影响因素分析及含气量测试方法[J].中国矿业,2015,24(12):80-85. YOU Shenggang,GUO Qian,GENG Xiaojin,et al.Factors affecting the shale gas content and gas content testing methods[J].China Mining Magazine,2015,24(12):80-85. [13] 郭少斌,黄磊.页岩气储层含气性影响因素及储层评价:以上扬子古生界页岩气储层为例[J].石油实验地质,2013,35(6):601-606. GUO Shaobin,HUANG Lei.Gas-bearing influential factors and evaluation of shale gas reservoir:A case study of Paleozoic shale gas reservoir in Upper Yangtze region[J].Petroleum Geology & Experiment,2013,35(6):601-606. [14] 万金彬,何羽飞,刘淼,等.页岩含气量测定及计算方法研究[J].测井技术,2015,39(6):756-761. WAN Jinbin,HE Yufei,LIU Miao,et al.Shale gas content measurement and calculation method[J].Well Logging Techno-logy,2015,39(6):756-761. [15] 吴艳艳,曹海虹,丁安徐,等.页岩气储层孔隙特征差异及其对含气量影响[J].石油实验地质,2015,37(2):231-236. WU Yanyan,CAO Haihong,DING Anxu,et al.Pore characteristics of a shale gas reservoir and its effect on gas content[J].Petroleum Geology & Experiment,2015,37(2):231-236. [16] 薛冰,张金川,杨超,等.页岩含气量理论图版[J].石油与天然气地质,2015,36(2):339-346. XUE Bing,ZHANG Jinchuan,YANG Chao,et al.Theoretical chart of shale gas content[J].Oil & Gas Geology,2015,36(2):339-346. [17] 梁红艺,谢小国,罗兵,等.煤层含气量评价方法研究与应用[J].特种油气藏,2016,23(3):44-47. LIANG Hongyi,XIE Xiaoguo,LUO Bing,et al.Coalbed methane content evaluation and application[J].Special OiL& Gas Re-servoirs,2016,23(3):44-47. [18] 俞凌杰,范明,蒋启贵,等.页岩气现场解吸方法优化[J].石油实验地质,2015,37(3):402-406. YU Lingjie,FAN Ming,JIANG Qigui,et al.Optimization of shale gas desorption method in field[J].Petroleum Geology & Experiment,2015,37(3):402-406. [19] 唐颖,张金川,刘珠江,等.解吸法测量页岩含气量及其方法的改进[J].天然气工业,2011,31(10):108-112. TANG Ying,ZHANG Jinchuan,LIU Zhujiang,et al.Use and improvement of the desorption method in shale gas content tests[J].Natural Gas Industry,2011,31(10):108-112. [20] 武瑾,王红岩,拜文华,等.渝东南龙马溪组页岩储层特征及吸附影响因素分析[J].断块油气田,2013,20(6):713-718. WU Jin,WANG Hongyan,BAI Wenhua,et al.Analysis on characteristics of Longmaxi Formation shale reservoir in southeast district of Chongqing and adsorption influence factor[J].Fault-Block Oil and Gas Field,2013,20(6):713-718. [21] 蒋官澄,范劲,李颖颖,等.新型促页岩气解吸附体系研究[J].特种油气藏,2014,21(3):116-119. JIANG Guancheng,FAN Jin,LI Yingying,et al.Study on new system used for acceleration of shale gas desorption[J].Special OiL& Gas Reservoirs,2014,21(3):116-119. [22] 邓泽,刘洪林,康永尚.煤层气含气量测试中损失气量的估算方法[J].天然气工业,2008,28(3):85-86. DENG Ze,LIU Honglin,KANG Yongshang.Estimation methods of lost gas in coal-bed gas content testing[J].Natural Gas Industry,2008,28(3):85-86. [23] 杨振恒,魏志红,何文斌,等.川东南地区五峰组-龙马溪组页岩现场解吸气特征及其意义[J].天然气地球科学,2017,28(1):156-163. YANG Zhenheng,WEI Zhihong,HE Wenbin,et al.Characteristics and significance of onsite gas desorption from Wufeng-Longmaxi shales in southeastern Sichuan Basin[J].Natural Gas Geoscience,2017,28(1):156-163. [24] 李玉喜,乔德武,姜文利,等.页岩气含气量和页岩气地质评价综述[J].地质通报,2011,30(2/3):308-317. LI Yuxi,QIAO Dewu,JIANG Wenli,et al.Gas content of gas-bearing shale and its geological evaluation summary[J].Geolo-gical Bulletin of China,2011,30(2/3):308-317.
点击查看大图
计量
- 文章访问数: 1140
- HTML全文浏览量: 79
- PDF下载量: 314
- 被引次数: 0