定量荧光技术在页岩油储层研究中的应用——以准噶尔盆地玛湖凹陷二叠系风城组为例

江程舟; 王贵文; 宋连腾; 黄立良; 王松; 张益粼; 黄玉越; 范旭强

doi:10.11781/sysydz2025030634

定量荧光技术在页岩油储层研究中的应用——以准噶尔盆地玛湖凹陷二叠系风城组为例

doi: 10.11781/sysydz2025030634

江程舟^{1, 2,},
王贵文^{1, 2, ,},
宋连腾³,
黄立良⁴,
王松^{1, 2},
张益粼⁵,
黄玉越^{1, 2},
范旭强⁶

1.
中国石油大学(北京) 地球科学学院, 北京 102249
2.
中国石油大学(北京) 油气资源与探测国家重点实验室, 北京 102249
3.
中国石油勘探开发研究院, 北京 100083
4.
中国石油新疆油田分公司勘探开发研究院, 新疆克拉玛依 834000
5.
中国石化勘探分公司物探研究院, 成都 610041
6.
中国石油经济技术研究院, 北京 100724

基金项目:

国家自然科学基金 41872133

中国石油—中国石油大学(北京)战略合作协议 ZLZX2020-01-05-03

详细信息

作者简介:
江程舟(1997—)，男，博士生，从事页岩油储层地质学研究。E-mail: jcz_cup@163.com

通讯作者:
王贵文(1966-), 男, 博士, 教授, 从事页岩油储层地质学研究。E-mail: wanggw@cup.edu.cn

中图分类号: TE135
计量
- 文章访问数: 30
- HTML全文浏览量: 8
- PDF下载量: 8
- 被引次数: 0
出版历程
- 收稿日期: 2024-07-17
- 修回日期: 2025-04-06
- 刊出日期: 2025-05-28

Quantitative fluorescence techniques and their applications in shale oil reservoir research: a case study of Permian Fengcheng Formation in Mahu Sag, Junggar Basin

JIANG Chengzhou^{1, 2
,},
WANG Guiwen^{1, 2
, ,},
SONG Lianteng³,
HUANG Liliang⁴,
WANG Song^{1, 2},
ZHANG Yilin⁵,
HUANG Yuyue^{1, 2},
FAN Xuqiang⁶

1.
College of Geosciences, China University of Petroleum (Beijing), Beijing 102249, China
2.
State Key Laboratory of Petroleum Resources and Prospecting, China University of Petroleum (Beijing), Beijing 102249, China
3.
Research Institute of Petroleum Exploration and Development, PetroChina, Beijing 100083, China
4.
Research Institute of Petroleum Exploration and Development, Xinjiang Oilfield Company, PetroChina, Karamay, Xinjiang 834000, China
5.
Geophysical Research Institute, SINOPEC Exploration Company, Chengdu, Sichuan 610041, China
6.
Economic and Technology Research Institute, PetroChina, Beijing 100724, China

摘要

摘要: 准噶尔盆地玛湖凹陷二叠系风城组页岩油储层具有源储一体的特征，其形成过程受沉积环境、成岩作用和有机质演化等多种因素的影响，导致其烃源岩性质和储层特征异常复杂。目前，无机矿物发育和有机质演化对储层或赋存页岩油性质所造成的影响尚不明确。针对上述问题，将已经广泛应用于常规储层研究的定量荧光技术，如储层萃取液定量荧光分析技术(QGF-E)和全息扫描荧光技术(TSF)等拓展到陆相页岩油储层研究中。将QGF-E和岩石热解相结合发现，热解参数游离烃(S₁)与QGF-E强度呈正相关，且变化范围较大，说明含油饱和度的大小主要受S₁的控制；TSF分析揭示，在其他检测条件相同的情况下，归一化的TSF光谱最大强度与二维核磁实验结果共同表明，页岩油密度(API)的差异与黏土矿物吸附的含羟基的重质组分密切相关，且黏土矿物含量越高，能够吸附的有机质越多；原油成熟度指标(R₁)进一步说明了原始沉积背景下，生烃母质的差异以及成岩改造后孔隙类型以及结构特征是影响储层中页岩油性质的关键因素。这些研究技术和方法可以作为沟通不同参数之间的“桥梁”，有助于进一步认识页岩油储层特征，为后续非常规油气的勘探开发提供参考。
- 含油饱和度 /
- 游离烃 /
- 原油性质 /
- 储层定量荧光技术 /
- 风城组 /
- 二叠系 /
- 玛湖凹陷 /
- 准噶尔盆地
Abstract: The shale oil reservoirs of the Permian Fengcheng Formation in the Mahu Sag of the Junggar Basin are characterized by a source and reservoir integration. Their formation process is affected by various factors, including sedimentation, diagenesis, and organic matter evolution, resulting in highly complex source rock properties and reservoir characteristics. Currently, the effects of inorganic mineral development and organic matter evolution on reservoir and shale oil properties remain unclear. To address these issues, this study extends the application of quantitative fluorescence (QF) techniques, which are widely used in conventional reservoir research, to continental shale oil reservoirs. Techniques such as quantitative grain fluorescence on extract (QGF-E) and total scanning fluorescence (TSF) were utilized. By combining QGF-E analysis and rock pyrolysis, it was found that free hydrocarbon (S₁) was positively correlated with QGF-E intensity, and their variation range was significant. This indicated that oil saturation was mainly controlled by S₁. Under the same testing conditions, the normalized TSF spectra's maximum intensity and two-dimensional nuclear magnetic resonance (2D NMR) experimental results showed that the differences in shale oil density (API gravity) were related to the adsorption of hydroxyl-rich heavy organic matter by clay minerals. Higher clay mineral content was found to adsorb more organic matter. The crude oil maturity index (R₁) further indicated that the differences in bio-precursors under the original depositional environment and the variations in pore types and structures after diagenetic alteration were key factors affecting the properties of shale oil in the reservoir. These analytical techniques and methods serve as a bridge connecting different parameters, facilitating a deeper understanding of the characteristics of the shale oil reservoir and providing valuable references for the exploration and development of unconventional oil and gas resources.
- oil saturation /
- free hydrocarbon /
- crude oil properties /
- reservoir quantitative fluorescence technique /
- Fengcheng Formation /
- Permian /
- Mahu Sag /
- Junggar Basin
注释:

利益冲突声明/Conflict of Interests

所有作者声明不存在利益冲突。

All authors declare no relevant conflict of interests.

作者贡献/Authors’Contributions

江程舟完成论文的撰写和修改；王贵文、黄立良、江程舟负责稿件的总体构思和数据分析；宋连腾负责实验设计；江程舟、王松、黄玉越、张益粼、范旭强参与图件绘制。所有作者均阅读并同意最终稿件的提交。

The manuscript was drafted and revised by JIANG Chengzhou. WANG Guiwen, HUANG Liliang, and JIANG Chengzhou were responsible for the overall conceptualization and data analysis of the manuscript. The experiment was designed by SONG Lianteng. JIANG Chengzhou, WANG Song, HUANG Yuyue, ZHANG Yilin, and FAN Xuqiang participated in figure drawing. All authors have read the final version of the paper and consented to its submission.

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图 1 准噶尔盆地玛湖凹陷构造位置及其地层综合柱状图

a.准噶尔盆地构造位置，修改自文献[25]；b.玛湖凹陷构造位置；c.研究区地层柱状图，修改自文献[26]。

Figure 1. Structural location and stratigraphic comprehensive histogram of Mahu Sag, Junggar Basin

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图 2 准噶尔盆地玛湖凹陷生烃母质分布及生烃演化模式

a.风城组一、二段碱湖生物—环境协同演化模式, 修改自文献[33]; b.风城组液态烃生烃演化特征, 修改自文献[34]。

Figure 2. Distribution of bio-precursors and hydrocarbon generation evolution model of Mahu Sag, Junggar Basin]。

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图 3 准噶尔盆地玛湖凹陷二叠系风城组X射线衍射分析结果

Figure 3. X-ray diffraction analysis results of Permian Fengcheng Formation, Mahu Sag, Junggar Basin

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图 4 准噶尔盆地玛湖凹陷二叠系风城组页岩岩相三角图修改自文献[36]。

Figure 4. Ternary plots of shale facies in Permian Fengcheng Formation, Mahu Sag, Junggar Basin

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图 5 准噶尔盆地玛湖凹陷二叠系风城组页岩QGF-E分析光谱

Figure 5. QGF-E spectral analysis of shale from Permian Fengcheng Formation, Mahu Sag, Junggar Basin

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图 6 准噶尔盆地玛湖凹陷二叠系风城组页岩TSF分析光谱

Figure 6. TSF spectral analysis of shale from Permian Fengcheng Formation, Mahu Sag, Junggar Basin

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图 7 准噶尔盆地玛湖凹陷二叠系风城组页岩二维核磁T₁—T₂图

Figure 7. 2D NMR T₁-T₂ diagrams of shale from Permian Fengcheng Formation, Mahu Sag, Junggar Basin

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图 8 准噶尔盆地玛湖凹陷二叠系风城组岩石热解—QGF-E参数交会图

Figure 8. Cross plots of rock pyrolysis and QGF-E parameters of Permian Fengcheng Formation, Mahu Sag, Junggar Basin

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图 9 准噶尔盆地玛湖凹陷二叠系风城组矿物含量—TSF参数交会图

Figure 9. Cross plots of mineral content and TSF parameters of Permian Fengcheng Formation, Mahu Sag, Junggar Basin

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表 1 准噶尔盆地玛湖凹陷玛页1井二叠系风城组岩样QGF-E、有机地化、XRD及含油饱和度数据

Table 1. QGF-E, organic geochemistry, XRD, and oil saturation data for rock samples from Permian Fengcheng Formation of well MY1, Mahu Sag, Junggar Basin

样品编号	深度/m	QGF-E/pc	λ/nm	ω(TOC)/%	S₁/(mg/g)	S₂/(mg/g)	矿物含量/%					含油饱和度/%
样品编号	深度/m	QGF-E/pc	λ/nm	ω(TOC)/%	S₁/(mg/g)	S₂/(mg/g)	石英	长石	方解石	白云石	黄铁矿	含油饱和度/%
1	4 716.34	8 671.8	376.0	0.83	0.88	1.09	13.5	16.2	14.5	48.0	3.6	55
2	4 720.15	6 911.6	378.0	0.67	0.65	1.02	46.5	9.6	1.8	37.7	1.6	38
3	4 720.29	11 822.8	374.0	0.49	1.07	1.02	28.8	9.9	39.5	16.6	1.2	61
4	4 721.06	9 555.8	378.0	0.54	0.59	0.95	17.9	13.7	27.5	34.0	2.0	73
5	4 766.56	9 915.5	380.0	0.72	0.97	1.42	41.5	13.2	0.0	38.7	3.0	69
6	4 773.86	10 118.2	379.1	1.19	0.77	3.54	10.8	42.9	24.3	10.6	7.6	60
7	4 800.45	9 763.6	378.0	0.54	0.35	1.47	39.4	7.3	0.5	49.3	1.2	52
8	4 813.65	8 402.9	381.1	0.57	0.10	1.70	24.3	7.9	17.4	43.3	3.8	53
9	4 835.28	6 110.1	381.1	1.04	0.12	0.87	25.1	12.8	0.0	50.4	4.3	36
10	4 840.37	6 440.8	377.1	0.63	0.12	1.51	24.5	38.9	0.0	17.8	7.2	40
11	4 842.99	4 450.1	377.1	0.59	0.33	0.93	40.7	8.5	5.3	40.8	1.8	21
12	4 847.21	3 928.3	377.1	0.97	0.21	1.25	24.7	35.7	0.0	26.7	8.1	19
13	4 850.35	4 377.1	382.0	1.59	0.12	1.78	39.5	10.9	26.8	8.4	5.5	23
14	4 853.35	7 141.8	378.0	0.70	0.38	1.25	23.0	11.3	0.0	53.9	5.5	40

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表 2 准噶尔盆地玛湖凹陷玛页1井二叠系风城组页岩TSF及XRD数据

Table 2. TSF and XRD data for shale in Permian Fengcheng Formation of well MY1, Mahu Sag, Junggar Basin

样品编号	深度/m	Max-Em/nm	Max-Ex/nm	归一化的TSF Max/pc	R₁	R₂	长石/%	白云石/%	黏土矿物/%
a	4 738.73	304	409	7 292.3	7.308	10.355	15.3	40.6	7.5
b	4 740.43	260	375	8 529.1	5.602	8.301	16.8	33.8	6.4
c	4 744.90	260	380	6 957.3	5.206	7.772	19.6	28.2	2.5
d	4 751.36	302	407	9 692.7	7.700	11.082	8.2	50.5	9.9
e	4 759.42	260	380	5 484.4	6.262	8.875	8.2	52.0	4.4
f	4 775.86	258	373	10 126.6	2.790	4.237	64.8	19.9	3.1
g	4 790.94	262	377	5 772.9	4.694	6.791	39.5	24.6	2.9
h	4 799.67	270	380	7 492.8	5.981	8.528	6.4	52.8	3.1
i	4 804.95	260	380	11 885.9	5.225	7.474	47.2	13.9	8.6
j	4 830.31	262	382	6 296.2	5.353	7.722	28.6	32.6	5.7
k	4 850.43	260	375	15 094.3	4.828	6.862	30.9	13.5	9.2
l	4 851.11	262	382	9 218.8	6.145	8.349	30.1	11.8	7.0

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